Starting as a new student - Revision history

Fveldhuizen: Added ppt for new SOC members

2026-04-02T09:51:46Z

Added ppt for new SOC members

← Older revision		Revision as of 09:51, 2 April 2026
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	There are a few things you will have to take care of yourself, preferably before starting the internship:		There are a few things you will have to take care of yourself, preferably before starting the internship:
	* Obtaining a '''Radboud campus card''' with an S/U/E number. If you do not have such a card yet and are not a student from the Radboud, you can contact sa@dpo.ru.nl with your request. They will want a picture from you for on the campus card. They will contact you when you can pick it up (used to be at the Erasmus building (E 19.02).		* Obtaining a '''Radboud campus card''' with an S/U/E number. If you do not have such a card yet and are not a student from the Radboud, you can contact sa@dpo.ru.nl with your request. They will want a picture from you for on the campus card. They will contact you when you can pick it up (used to be at the Erasmus building (E 19.02).
	* A '''science account''', which you can get from C&Cz as a student or they are applied for by Marieke to C&Cz. You will need this account in order to access the VPN and get your mass/NMR spectra. A guide for obtaining a science account is found at [https://cncz.science.ru.nl/en/howto/login/ here].		* A '''science account''', which you can get from C&Cz as a student or they are applied for by Marieke to C&Cz. You will need this account in order to access the VPN and get your mass/NMR spectra. A guide for obtaining a science account is found at [https://cncz.science.ru.nl/en/howto/login/ here]. <br/>
			See also [[Media:Presentation for new SOC members.pptx\|Presentation for new SOC members]].
	=The mandatory stuff=		=The mandatory stuff=
	== Registration & Access to the wings ==		== Registration & Access to the wings ==

Fveldhuizen: /* Going into the lab */

2025-04-07T09:49:10Z

Going into the lab

← Older revision		Revision as of 09:49, 7 April 2025
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	* Obtain the relevant '''safety equipment''' such as a lab coat and safety goggles. These can be obtained from {{Technician mercator}} for working in Mercator and {{Technician huygens}} for working in Huygens.		* Obtain the relevant '''safety equipment''' such as a lab coat and safety goggles. These can be obtained from {{Technician mercator}} for working in Mercator and {{Technician huygens}} for working in Huygens.
	* Obtain a '''physical lab journal''' (in addition to pencils and other office supplies) which can be acquired from the secretary office in Hg and from {{Technician mercator}} in M3.		* Obtain a '''physical lab journal''' (in addition to pencils and other office supplies) which can be acquired from the secretary office in Hg and from {{Technician mercator}} in M3.
	* Gain access to the '''electronic lab notebook (ELN)''' for which we currently use [https://chemotion.science.ru.nl/home ~~chemotion~~]. Daniel Blanco-Ania is the responsible ~~person~~ for this and can give you access. Hence, send an email to him or pass by his office. '''Important:''' as a student you need to share your ELN with your supervisor and you should close experiments after 3 weeks of completing them. A more extensive guide on using Chemotion can be found [https://docs.google.com/document/d/1wdaeXOB5fZVcQ8pyIDBOKXN5hEscbM5El8OwFzIN1Jw/edit here]. The minimal requirements according to the Boltje lab of ELN recording are found [[Chemotion#ELN minimal book keeping\| here]].		* Gain access to the '''electronic lab notebook (ELN)''' for which we currently use [[Chemotion]]. Chemotion can be accessed [https://chemotion.science.ru.nl/home here]. Daniel Blanco-Ania is the person responsible for this and can give you access. Hence, send an email to him or pass by his office. '''Important:''' as a student you need to share your ELN with your supervisor and you should close experiments after 3 weeks of completing them. A more extensive guide on using Chemotion can be found [https://docs.google.com/document/d/1wdaeXOB5fZVcQ8pyIDBOKXN5hEscbM5El8OwFzIN1Jw/edit here]. The minimal requirements according to the Boltje lab of ELN recording are found [[Chemotion#ELN minimal book keeping\| here]].

	== Lab equipment access ==		== Lab equipment access ==

Fveldhuizen: /* Full characterization of a NCE */

2025-04-07T09:29:23Z

Full characterization of a NCE

← Older revision		Revision as of 09:29, 7 April 2025
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	===Full characterization of a NCE===		===Full characterization of a NCE===
			TLC, NMR, and HRMS are mandatory for new compounds.<br/>
	~~(to~~ be ~~filled)..~~.		An infrared spectrum can be made if the structure is unclear from NMR and HRMS, and is necessary for publication.

	== How to behave in the lab ==		== How to behave in the lab ==

Fveldhuizen: /* MS access */

2025-04-07T09:25:44Z

MS access

← Older revision		Revision as of 09:25, 7 April 2025
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	There are various mass spectrometers available to SOC but most students will only manually operate the ISQs. The ISQ in Huygens (HG03.411) is a MS for pure samples only, while the ISQ in Mercator is a LC-MS, for analyzing mixtures. A guide on how to operate the ISQs can be found [https://gitlab.science.ru.nl/jzelenka/isq/-/blob/master/README.md here], which you will need to read prior to getting training for the ISQs. After measuring your MS samples, you can retrieve the results either directly from the computers or via \\msspectra-srv.science.ru.nl\msspectra by adding this external drive to your pc and access via your science account.<br/>		There are various mass spectrometers available to SOC but most students will only manually operate the ISQs. The ISQ in Huygens (HG03.411) is a MS for pure samples only, while the ISQ in Mercator is a LC-MS, for analyzing mixtures. A guide on how to operate the ISQs can be found [https://gitlab.science.ru.nl/jzelenka/isq/-/blob/master/README.md here], which you will need to read prior to getting training for the ISQs. After measuring your MS samples, you can retrieve the results either directly from the computers or via \\msspectra-srv.science.ru.nl\msspectra by adding this external drive to your pc and access via your science account.<br/>
	The current mass tutors are Daan Hamstra and Robin Schenker for the ISQ in Huygens, and Robin Schenker and Enebie Ramos Caceres for the ISQ in Mercator 3.		The current mass tutors are Daan Hamstra and Robin Schenker for the ISQ in Huygens, and Robin Schenker and Enebie Ramos Caceres for the ISQ in Mercator 3.

			==== HRMS ====
			High resolution mass spectrometry (HRMS) is used to obtain high quality mass spectra. This is not necessary for every sample, but only for important compounds and when lower resolution measurements are unclear. <br/>
			Jan Zelenka is in charge of measuring HRMS. These measurements typically take place once a month. Before each measurement, Jan will send round an email asking people to submit samples.

	=== Other equipment ===		=== Other equipment ===

Fveldhuizen: /* MS access */

2025-04-07T09:13:39Z

MS access

← Older revision		Revision as of 09:13, 7 April 2025
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	=== MS access ===		=== MS access ===
	There are various mass spectrometers available to SOC but most students will only manually operate the ISQs. The ISQ in Huygens (HG03.411) is a MS for pure samples only, while the ISQ in Mercator is a LC-MS, for analyzing mixtures. A guide on how to operate the ISQs can be found [https://gitlab.science.ru.nl/jzelenka/isq/-/blob/master/README.md here], which you will need to read prior to getting training for the ISQs. After measuring your MS samples, you can retrieve the results either directly from the computers or via \\msspectra-srv.science.ru.nl\msspectra by adding this external drive to your pc and access via your science account.<br/>		There are various mass spectrometers available to SOC but most students will only manually operate the ISQs. The ISQ in Huygens (HG03.411) is a MS for pure samples only, while the ISQ in Mercator is a LC-MS, for analyzing mixtures. A guide on how to operate the ISQs can be found [https://gitlab.science.ru.nl/jzelenka/isq/-/blob/master/README.md here], which you will need to read prior to getting training for the ISQs. After measuring your MS samples, you can retrieve the results either directly from the computers or via \\msspectra-srv.science.ru.nl\msspectra by adding this external drive to your pc and access via your science account.<br/>
	The current mass tutors are Daan Hamstra and Robin Schenker for the ISQ in Huygens, and Enebie Ramos Caceres for the ISQ in Mercator 3.		The current mass tutors are Daan Hamstra and Robin Schenker for the ISQ in Huygens, and Robin Schenker and Enebie Ramos Caceres for the ISQ in Mercator 3.

	=== Other equipment ===		=== Other equipment ===

Fveldhuizen: /* MS access */

2025-04-07T09:13:08Z

MS access

← Older revision		Revision as of 09:13, 7 April 2025
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	=== MS access ===		=== MS access ===
	There are various mass spectrometers available to SOC but most students will only manually operate the ISQs. A guide on how to operate the ISQs can be found [https://gitlab.science.ru.nl/jzelenka/isq/-/blob/master/README.md here], which you will need to read prior to getting training for the ISQs. After measuring your MS samples, you can retrieve the results either directly from the computers or via \\msspectra-srv.science.ru.nl\msspectra by adding this external drive to your pc and access via your science account.<br/>		There are various mass spectrometers available to SOC but most students will only manually operate the ISQs. The ISQ in Huygens (HG03.411) is a MS for pure samples only, while the ISQ in Mercator is a LC-MS, for analyzing mixtures. A guide on how to operate the ISQs can be found [https://gitlab.science.ru.nl/jzelenka/isq/-/blob/master/README.md here], which you will need to read prior to getting training for the ISQs. After measuring your MS samples, you can retrieve the results either directly from the computers or via \\msspectra-srv.science.ru.nl\msspectra by adding this external drive to your pc and access via your science account.<br/>
	The current mass tutors are Daan Hamstra and Robin Schenker for the ISQ in Huygens, and Enebie Ramos Caceres for the ISQ in Mercator 3.		The current mass tutors are Daan Hamstra and Robin Schenker for the ISQ in Huygens, and Enebie Ramos Caceres for the ISQ in Mercator 3.

Fveldhuizen: /* Lab equipment access */

2025-04-04T10:58:30Z

Lab equipment access

← Older revision		Revision as of 10:58, 4 April 2025
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	==== Purification equipment ====		==== Purification equipment ====
	<div class="toccolours mw-collapsible" style="width:600px; overflow:auto;">		<div class="toccolours mw-collapsible mw-collapsed" style="width:600px; overflow:auto;">

	===== Preparative HPLC =====		===== Preparative HPLC =====
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	==== Analysis equipment ====		==== Analysis equipment ====

	<div class="toccolours mw-collapsible" style="width:600px; overflow:auto;">		<div class="toccolours mw-collapsible mw-collapsed" style="width:600px; overflow:auto;">

	===== IR =====		===== IR =====
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	==== Synthesis equipment ====		==== Synthesis equipment ====

	<div class="toccolours mw-collapsible" style="width:600px; overflow:auto;">		<div class="toccolours mw-collapsible mw-collapsed" style="width:600px; overflow:auto;">

	===== Synthesis microwave =====		===== Synthesis microwave =====

Fveldhuizen at 11:05, 2 April 2025

2025-04-02T11:05:54Z

← Older revision		Revision as of 11:05, 2 April 2025
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	There are a few things you will have to take care of yourself, preferably before starting the internship:		There are a few things you will have to take care of yourself, preferably before starting the internship:
	* Obtaining a '''Radboud campus card''' with an S/U/E number. If you do not have such a card yet and are not a student from the Radboud, you can contact sa@dpo.ru.nl with your request. They will want a picture from you for on the campus card. They will contact you when you can pick it up (used to be at the Erasmus building (E 19.02).		* Obtaining a '''Radboud campus card''' with an S/U/E number. If you do not have such a card yet and are not a student from the Radboud, you can contact sa@dpo.ru.nl with your request. They will want a picture from you for on the campus card. They will contact you when you can pick it up (used to be at the Erasmus building (E 19.02).
	* A '''science account''', which you can get from C&Cz as a student or they are applied for by Marieke to C&Cz. You will need this account in order to access the VPN and get your mass/NMR spectra. A guide for obtaining a science account is found at [https://cncz.science.ru.nl/en/howto/login/ here]~~. If you are reading this page from the Wiki than the Science account corresponds to the SAML login you used to access this wiki~~.		* A '''science account''', which you can get from C&Cz as a student or they are applied for by Marieke to C&Cz. You will need this account in order to access the VPN and get your mass/NMR spectra. A guide for obtaining a science account is found at [https://cncz.science.ru.nl/en/howto/login/ here].
	=The mandatory stuff=		=The mandatory stuff=
	== Registration & Access to the wings ==		== Registration & Access to the wings ==

Fveldhuizen at 09:16, 28 March 2025

2025-03-28T09:16:26Z

← Older revision		Revision as of 09:16, 28 March 2025
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	===MestreNova===		===MestreNova===
	MestreNova is a licensed software with which we can analyze recorded NMR-spectra. MestreNova can be obtained from the [https://cncz.science.ru.nl/en/howto/install-share/ install network drive of CnCz], where also an install guide is found.		MestreNova is a licensed software with which we can analyze recorded NMR-spectra. MestreNova can be obtained from the [https://cncz.science.ru.nl/en/howto/install-share/ install network drive of CnCz], where also an install guide is found.

			== When leaving the lab ==
			When finished with your internship, it is important to leave the lab in a good state, and the data of your experiments should be stored properly. Use the checklist below to make sure you do not miss anything. <br/>
			[[Media:Leaving the lab - To do list interns.pdf \| Leaving the lab Checklist]]

	=Other useful but non-mandatory things=		=Other useful but non-mandatory things=

Fveldhuizen: /* Lab equipment access */

2025-03-27T11:27:35Z

Lab equipment access

← Older revision		Revision as of 11:27, 27 March 2025
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	==== NMR in Huygens ====		==== NMR in Huygens ====
	There are two NMRs in wing 4, floor 3 of the Huygens building: a 400 MHz and a 500 MHz. The 400 is always in automation mode, which means you add your sample to a queue, and it will measure your sample automatically. To minimize the waiting time during the day your experiments cannot be longer than 10 minutes. If they are, you will have to measure them during the night, either on the 400 or 500.<br/>		There are two NMRs in wing 4, floor 3 of the Huygens building: a 400 MHz and a 500 MHz. The 400 is always in automation mode, which means you add your sample to a queue, and it will measure your sample automatically. To minimize the waiting time during the day your experiments cannot be longer than 10 minutes. If they are, you will have to measure them during the night, either on the 400 or 500.<br/>
	The 500 is not in automation mode during the day and ~~will be~~ available for students ~~only for the night queue~~. <br/>		The 500 is not in automation mode during the day and typically not available for students. <br/>
	Please ask for training before using.<br/>		Please ask for training before using.<br/>
	Training: Nuwanthika Kumarage.		Training: Nuwanthika Kumarage.
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	<div class="toccolours mw-collapsible" style="width:600px; overflow:auto;">		<div class="toccolours mw-collapsible" style="width:600px; overflow:auto;">

	===== Synthesis microwave ~~(currently out of order)~~ =====		===== Synthesis microwave =====
	Can be used to initiate reactions.<br/>		Can be used to initiate reactions at high temperature.<br/>
	Training: ?<br/>		Training: Frank Veldhuizen?<br/>

	===== Autoclave =====		===== Autoclave =====